• 专利附录
  • 专利说明
  • 权利要求
  • 类似技术
  • 同族专利
  • 引用文献
  • 法律状态
  • 优先权
    • 专利摘要:
    1513977 Tobacco substitutes PHILIP MORRIS INC 13 Aug 1976 [15 Aug 1975] 33878/76 Heading A2C [Also in Division C3] A film forming carbohydrate which has been treated with ozone so that it has at least 0.2 milliequivalent of carboxyl groups per gram is employed as a smoking material. The carbohydrate is preferably a polysaccharide such as the pectin contained in lemon albedo. The smoking material may be mixed with tobacco or used alone. Other conventional ingredients such as flavourants, humectants and burn additives may be added.
    公开号:SU728689A3
    申请号:SU762388101
    申请日:1976-08-16
    公开日:1980-04-15
    发明作者:Б.Рэйнер Норман；Б.Хоуелзел Чарльз；С.Гопкинс Вильям
    申请人:Филип Моррис Инкорпорейтед (Фирма)；
    IPC主号:
    专利说明:

    one
    The invention relates to a technique for producing a smoking product used as a filler or wrapping material in the manufacture of smoking articles.
    A method of producing a smoking product is known, which involves casting a layer of film-forming carbohydrate material to the surface, then drying to form a solid film and cutting the latter.
    However, the smoking product obtained in a known manner, when tested in smoking articles, produces a less pleasant taste and more caustic and sharp smoke than most Tobacco.
     The smoking product does not withstand processing and molding during the production of smoking articles.
    In addition, the smoking material is crushed, turning into particles or dust, does not have the corresponding durability and strength when used without wrinkling in smoking articles.
    The aim of the invention is to improve the quality of the product.
    This is achieved by the fact that, in the proposed method for producing a smoking product, the carbohydrate material is treated with ozone or a gaseous mixture containing ozone, until a carbohydrate group is formed in the carbohydrate material 0.2-0.8 meq per gram of carbohydrate material.
    In this case, the processing of the carbohydrate material with ozone is carried out before the casting process.
    In addition, the processing of the carbohydrate material with ozone is carried out after the cutting process.
    Treatment with ozone is carried out at. 0-90 C.
    At the same time, the gaseous mixture used in the processing of carbohydrate material contains 2-10% ozone and 90-98% by volume of gas selected from the group comprising air and oxygen.
    As the film-forming carbohydrate material polysaccharide is used,. preferably pectin.
    In addition, lemon albedo is used as a film-forming carbohydrate material.
    The method is carried out as follows.
    The film-forming carbohydrate material is treated with ozone or
    a gaseous mixture containing oEoI, preferably in the form of a finely divided or porous product, to ensure the greatest possible surface temperature of contact with ozone.
    As a film-forming carbohydrate material, polysaccharides are used, preferably with a relatively high 4-molecular weight, which can be considered polymers that are suitable for reproducing proteins from gluco- or fructorazone rings or their mixtures and which are sufficiently strong when casting with: a liquid carrier of the film.
    . ; I use pectin as a polysaccharide (in the form of complex methyl
    ether) with the formula (, "OS), where p; 100-2000.
    : Pectins can be vegetables and fruits, in particular, dsKTHH extracted from fruits or vegetables, or the pectin containing fruit component of the albedo of a lemon, is used.
    In addition, other natural polysaccharide substrate-forming materials can be used, including pectins or algins, as well as natural galactomal film-forming materials, including Phobian Robinia resin or guarose resin, These film-forming materials are suitable for casting from aqueous solutions of suspensions and most of them are solvents water.
    The crushed polysaccharide is placed in the reactor mill container, while the moisture content of the polysaccharide should be at the level of 5-80 weight,% based on the total weight of the wet polysaccharide, preferably 10-35%,
    The container is preferably a fixed tower and should provide sufficient contact between the polysaccharide and the ozone.
    The polysaccharide is packaged in a container uniformly and loosely to form an interconnected network of voids in the duct of the introduced gas mixture.
    With uniform packaging container. a polysaccharide of odnothe or uniform size is used to prevent gravimetric sedimentation and the associated effect of the formation of percolation channels,
    With uneven or too dense packaging of the polysaccharide in a container, it is fluffed up using mechanical means or air.
    moisture content, as well as wet steam during its dryness.
    Gas is supplied at the bottom of the container. or in its upper part, and the container must have a device for) recycling the waste gas mixture, collecting it after processing, reactivation and injection back into the processing system for additional use,
    3 case of treatment of the floor; ca. arid gas containing an ozone containing state ozone contains 2-10% ozone and 90-98% o6beNry gas selected from the group comprising air and oxygen
    Ozone treatment And. gg of a mixture of wires at 0–90, preferably at 10–40 ° C, until the formation of carbohydrate material 0.2–0.8 mEq: sarboxy: 1 groups per gram of carbohydrate mother al a,
    In case the treatment temperature is lower, the rate of interaction of the ozone with the polysaccharide decreases.
    At a temperature of more than 10 ° C, the moisture content decreases, and therefore the content of dust and fine particles may increase, which leads to other forms of cleavage of the polysaccharide,
    to,
    Next, the polysaccharide treated with ozone removes the is3 container and ра, extracts or D1 sperg1 In liquid. The total content of the substance is 2--40, preferably 5-20%,%, and cast on the surface of the drying in the form of a thin layer. After that, the layer is heated and dried to form a solid resin.
    The ozone-treated polysaccharide fluid may contain various jjtr additives to improve the physical characteristics of the film or to convert the final product into a smoking material, such as magnesium carbonate or calcium carbonate, oxides, hydroxides, calcium and / or magnesium chlorides or phosphates, or pyrophosphates. gender and phosphate id, gi, calcium proxyapatite or / and magnesium. The alkaline earth metal compound can also be in the form of a salt of an organic acid, for example citrate, lactate, calcium carbonate or magnesium.
    Additives in an amount of 0-60. based on 100 hours polysaccharide, preferably - 40 weight.h, per 100 weight "h" of the polysaccharide
    The liquid containing the ozone-treated polysaccharide may include a plasticizer dd to impart the required properties of the whole composition in an amount up to 5 parts by weight per 100 weight, h, polysaccharide, and so: ke uvla / knitel, for example glycerin, mono acetyl 1liderol , triethylene glycol, invert sugar and grain syrup, in the amount of 2-40 weight, h, per 100 weight.h, polysaccharide. The total amount of sacifier and / or humidifier should not exceed 50 weight.h. per 100, polysaccharide
    It is also possible to use extracts of Izvistyev tobacco and other flavors, such as licorice, essential oils of rum, chocolate.
    The resulting film; the film is crushed or cut to the desired size depending on its use in smoking products. The polysaccharide can be treated with ozone also after dissolution or dispersion in a liquid (water). In this case, a sludge slurry solution is prepared with a total solids content of 4-15 wt.% And treated with a gaseous mixture containing 2-10 wt.% Of ozone by bubbling the gas mixture with a liquid through a liquid until at least 0.2 meq in the carbohydrate material carboxyl groups at .1 g. Process temperature 10–50 s. The polysaccharide can also be treated with ammonia, both before and after ozone treatment. The presence of ammonia increases the solubility of the ozone-treated polysaccharide and improves the taste characteristics in the case of using an aqueous solution of ammonia in the preparation of the casting mixture for casting a layer of carbohydrate material. The crushed polysaccharide is also treated with ozone at 40 to 10 minutes to 5 hours. Heat treatment accelerates the oxidative and hydrolytic reactions caused by treatment with ozone, and leads to a decrease in molecular weight while increasing the soluble polysaccharide and improving smoking qualities. Example 1. A granulated material obtained from an albedo obtained from lemon peels by removing the top layer of the skin and processing the remaining material by extraction to remove oleophilic oils, 50 g of lemon albedo is loaded into a 50.8 m diameter glass cylinder with a porous glass base with the formation of a column. with a height of 33.02 cm. Ozone is blown through a layer of lemon albedo for 30 minutes at atmospheric pressure, and approximately 145 liters of gas, containing 6% of ozone, pass through. The column is then purged with oxygen for 30 minutes to remove a trace of ozone. 10 g of ozone-treated albed lemon and 1.6 g of citric acid are mixed in 200 ml of hot water, acidified to pH 1.5 with concentrated hydrochloric acid. Next, the mixture is heated to and stirred for 15 minutes, then the mixture is cooled and neutralized with ammonium hydroxide, and then the following ingredients are added with continuous stirring (g): The re-precipitated carcass. Calcium Bonate .3.0 Grain Syrup 3.0 Glycerin 1.2 Sodium citrate-0.8 Sorbitol Potassium 0.2 Mixture viscosity is 5300 cP at room temperature, at a pressure of 5.2% by weight solid substances. Then the solutions of lemon albedo treated and ore-treated albedo are cast on stainless steel plates, using a doctor's leuvia with a gap of 0.635 mm, and drying out before the formation of films. The film obtained from the ozone-treated sample has a tensile strength of 0.098 kg / cm, and the strength of the control sample is 0.196 kg / cm. Then both films are cut in a cavity with a length of 12.7-25.4 mm, a width of 0.084 cm, and a thickness of 0.076.2-0.127 mm. To compare the nature of the smoke, cigarettes are prepared from processed and untreated albedo lemon by hand, and it has been found that the smoke from cigarettes containing ozone-treated albedo is more pleasant and better than from cigarettes made from untreated material. Example 2. To obtain a material with 14.4% solids, the following components are taken (parts by weight): calcium carbonate 33.0; HCMC (7 HS-FA HercuEes) cellulose, having a degree of substitution of 0.7 and a molecular weight such that a 1% solution of its sodium salt has a viscosity of 1300-2000 cP, 22.0; magnesium hydroxide 13.0; spent hops 11.0, successively extracted with hexane and ethyl alcohol and containing 14% pectin and 21% hemicellulose; cocoa 5.5; glycerin 5.5; o1-cellulose 3,3 potassium hydroxide 3,3; urea 2,2; boxing dye (annato, dye-used for butter) 1.2. Sludge viscosity at 25 ° C 3800 сP. The sludge will be placed in a cylindrical vessel with an inner diameter of 76.2 mm and treated with ozone, bubbling a gas mixture containing 8 vol.% Of ozone and 92 vol.% Oxygen through it, at 60 C for 5 hours. At the end of the treatment, the viscosity of the sludge is 16,000 cps. Next, the sludge is used to cast a layer of film-forming material, as described in Example 1, the film has a thickness of 0.1016 MiM and a tensile strength of 0.157 kg / cm. The film is cut and mixed with equal portions of natfal tobacco. The mixture is used to make cigarettes. The smoking qualities of these cigarettes are compared with the control ones made from an ozone untreated material, while the ozone treated cigarettes are softer and more pleasant. Example 3. 100 g of amypas, a derivative of cereal starch, are mixed with water to form a film of uv.pevodnogo material, as described in a greater 1.
    The film thickness is 0.07–62 mm and the tensile strength is O, IV kg / cm.
    The film is cut into strips 25.4 mm long and 2.54 mm wide.
    About 50 g of the cut film is loaded with a jacketed column, the temperature is maintained and the material containing 3.5 o6 is treated. ozone with a gaseous mixture, which is moistened by bubbling through water at.
    The treatment is carried out 5 hours after; by titration it is established that the strips of material contain 0.7 mEq of carboxyl groups per 1 g of dry matter.
    The resulting material is mixed in an equal portion of tobacco and the mixture is used to make cigarettes.
    Compared to the controls, these cigarettes produce softer and smoky smoke.
    Example 4. 50 g of amylopectin ama; 1steam at 15 ° C with water and through
    the mixture was bubbled for 6 h with a gaseous mixture with 3.5 vol.% of ozone at 35 ° С,
    The starch thus treated contains 0.8 mEq of carboxyl groups per gram of dry starch. A: The-treated material is then cast to form a film layer: as described in example 1, obtaining a film with a thickness of 0.1143 mm and a tensile strength of 0.196 kg / cm.
    The cut film material is mixed with a nat-ural cutted sheet in a 2: 3 ratio, and cigarettes are made from this mixture.
    When testing cigarettes, it was found that, compared with the controls, they produce softer and more pleasant smoke when smoking.
    Example 5. 50 g of albedo lemon, as in example 1, with a moisture content of 10.5% is mixed with 39.5 g of water in a plastic bag and held for an equilibrium of 24 hours, after which the moisture content is 50 wt.% Based on on the total weight of wet lemon juice. The material is then placed in a column with an inner diameter of 42 mm and formed from a glass disk. Height of loading is 190 mm.
    The gaseous mixture with B vol.% Of ozone obtained using a generator with a corona discharge, passes through a bubbler and then through a column. The exothermic reaction, accompanied by bleaching, starts from the bottom and advances stepwise to the top of the column. After 1 h, the generator is turned off, after h-3 h rinsed through; column dry air.
    The sample prepared in this way is used in the form of a casting isham, as described in Example 1, while the viscosity of the slurry is
    1500 cP with a content of 6.7% solids, and a control sample with the same concentration of solids has a viscosity of 11,400 cP.
    Both materials are cut and made cigarettes. When tested, the treated material produces smoother smoke than the control sample.
    The smoking product obtained by the proposed method can be used in the production of smoking products as a wrapping material for the latter and individual filler or in a mixture with tobacco in any proportions (with both natural and reconstructed tobacco), as well as in a mixture with one or more substitute mi tobacco.
    The proposed method is simple to implement, effective and economical.
    The resulting smoking product has high smoking qualities and some desirable properties of natural tobacco.
    权利要求:
    Claims (8)
    [1]
    1. A method for producing a smoking product, comprising casting a layer of film-forming carbohydrate material onto the surface, followed by drying to form a solid. films and cutting of the latter, characterized in that, in order to improve the quality of the product obtained, the carbohydrate material is treated with ozone or a gaseous mixture containing ozone to form carboxyl groups per 0.2 g of carbohydrate material in the carbohydrate material.
    [2]
    2. Method POP.1, differing in use and the fact that the processing of carbohydrate material with ozone is carried out before the casting process,
    [3]
    3. Method POP 1, characterized in that the processing of the carbohydrate material with ozone is carried out after the cutting process.
    [4]
    4. The method according to claims 1 to 3, which is also due to the fact that the gaseous mixture used to process the carbohydrate material contains 2-10% ozone and 90-98% by volume of gas selected from the group comprising air and oxygen.
    [5]
    5. The method according to claims 1 to 3, characterized in that the ozone treatment is carried out at 0-90 C.
    [6]
    6. The method according to claims 1 to 3, characterized in that a polysaccharide is used as a film-forming carbohydrate material.
    [7]
    7. The method according to claim 5, distinguishing and and with that. What is used as a polysaccharide pectin.
    9.72.f, S910
    [8]
    8. The method according to PP, 1-3, about tl and-Sources of research.
    due to the fact that, as a matter of fact,
    film-forming carbohydrate ma-1. ate (T SIL "3529602
    teriala use albedo lemon. 13.1-, publ. 1974.
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    同族专利:
    公开号 | 公开日
    GB1513977A|1978-06-14|
    US4034764A|1977-07-12|
    DE2636597A1|1977-02-17|
    AU1689176A|1978-02-23|
    CH625945A5|1981-10-30|
    US4143666A|1979-03-13|
    AU505262B2|1979-11-15|
    DE2636597B2|1981-01-22|
    引用文献:
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    法律状态:
    优先权:
    申请号 | 申请日 | 专利标题
    US05/604,944|US4034764A|1975-08-15|1975-08-15|Smoking material and method for its preparation|
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